Inorganic Chemistry Practical-I - CHE-306-MJP

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CHE – 306 – MJ – P Inorganic Chemistry Practical I, under faculty of Science and Technology, Savitribai Phule Pune University, Pune, according to new syllabus implemented from year 2026-27,...

Name : Inorganic Chemistry Practical-I - CHE-306-MJP
Vendor : Prashant Publication
Type : T.Y.B.Sc. | Sem. IV | CHE 306-(MJP)
Manufacturing : October 2026
Total Pages : 96 Pages

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INTERNATIONAL	XS	S	M	L	XL	XXL	XXXL
EUROPE	32	34	36	38	40	42	44
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CHEST FIT (INCHES)	28"	30"	32"	34"	36"	38"	40"
CHEST FIT (CM)	716	76	81	86	91.5	96.5	101.1
WAIST FIR (INCHES)	21"	23"	25"	27"	29"	31"	33"
WAIST FIR (CM)	53.5	58.5	63.5	68.5	74	79	84
HIPS FIR (INCHES)	33"	34"	36"	38"	40"	42"	44"
HIPS FIR (CM)	81.5	86.5	91.5	96.5	101	106.5	111.5
SKORT LENGTHS (SM)	36.5	38	39.5	41	42.5	44	45.5

CHE – 306 – MJ – P Inorganic Chemistry Practical I, under faculty of Science and Technology, Savitribai Phule Pune University, Pune, according to new syllabus implemented from year 2026-27, as per National Education Policy – 2020.
This book is written as per New syllabus introduced from 2026-27. We have tried to explain the concepts and information in easy language so that students could understand it easily. We feel that the information is presented in a simple form for the better understanding of students.
This book includes explanation for each point, number of illustrative examples are given and exercise is given at the end of each topic for the benefit of students. In our view the book will fulfil the expectations of students and teachers.

A. Gravimetric Estimations
• Experiment No. 1..........................................................................................7
Estimation of Fe as Fe2O3..

• Experiment No. 2........................................................................................10
Estimation of Calcium as Calcium Oxalate

• Experiment No. 3........................................................................................13
Estimation of Barium as Barium chromate.

• Experiment No. 4........................................................................................15
Estimation of Mg as Oxinate

• Experiment No. 5........................................................................................17
Estimation of Lead as Lead Chromate

• Experiment No. 6........................................................................................19
Estimation of Ba as BaSO4 using homogeneous precipitation method

• Experiment No. 7........................................................................................22
Estimation of Nickel as Ni – DMG.

• Experiment No. 8........................................................................................25
Analysis of sodium bicarbonate from mixture by thermal decomposition method.

• Experiment No. 9........................................................................................28
Determination of water of crystallization by thermal decomposition.

• Experiment No. 10......................................................................................31
Analysis of Food/Pharmaceutical sample for ash and sulphated ash: Aspirin.
B. Inorganic Preparations
Preparation of following inorganic complexes and spot tests for metal ions and ligands:

• Experiment No. 1........................................................................................35
Preparation of Trsi(acetylacetonato)iron(III) : [Fe(acac)3]

• Experiment No. 2........................................................................................38
Preparation of Hexaminecobalt(III) chloride : [Co(NH3)6]Cl3

• Experiment No. 3........................................................................................41 Preparation of Sodium Hexanitritocobaltate(III) : Na3[Co(NO2)6]

• Experiment No. 4........................................................................................44
Preparation of Potassium trioxalatoferrate(III) : K3[Fe(C2O4)3]

• Experiment No. 5........................................................................................48
Preparation of Trsi(acetylacetonato)manganese(III) : [Mn(acac)3]

• Experiment No. 6........................................................................................51
Peparation of Tris(glycinato)nickelate(II) : [Ni(gly)3]-

• Experiment No. 7........................................................................................54
Preparation of Potassium dioxalatocuprate(II): [Cu(C2O4)2]2-

• Experiment No. 8........................................................................................57
Preparation of Prussian Blue : KFe[Fe(CN)6]
C. Inorganic Qualitative Analysis

•Experiment No. 1........................................................................................63
Inorganic Qualitative analysis (5 mixtures)
[1 simple water soluble mixture, 2 mixtures containing borates and 2 mixtures containing phosphates] (Procedure from DST Manual ‘Green Chemistry’ Monograph must be followed strictly)

• Experiment No. 2........................................................................................81
Limit test for iron, chloride and sulphate from pharmaceutical raw materials.
OR

• Experiment No. 3........................................................................................84
Qualitative and confirmatory tests of inorganic toxicants of any four ions (Borate, copper, hypochlorite or nitrate or nitrite, Sb or Bi, Iodate, H2O2).