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the Handbook of Practical Chemistry in the hands of T.Y.B.Sc. students and the teachers of Chemistry. This handbook contains practicals of the three practical courses: Physical Chemistry Practical-I, Organic Chemistry...

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Practical Chemistry (Physical, Organic, Inorganic) CH-316, 317, 319
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the Handbook of Practical Chemistry in the hands of T.Y.B.Sc. students and the teachers of Chemistry. This handbook contains practicals of the three practical courses: Physical Chemistry Practical-I, Organic Chemistry Practical-I and Inorganic Chemistry Practical-I. This book has been written strictly according to the new revised syllabus of T.Y.B.Sc. Chemistry (2026) of Kavayitri Bahinabai Chaudhari North Maharashtra University, Jalgaon as per NEP 2020 Pattern.
The book focuses on understanding of the principle involved in different experiments. The experiments include the theory behind experiment, reactions involved, labelled diagrams, procedures, calculations, literature required and results. Preparation of solutions required for each experiment are given in details including quantity of reagents required. Procedures of experiments are simple and given in details considering level of students. Calculations are also given in details. Precautions required while performing some practicals are also given wherever necessary. Diagrams are well labelled for better understanding of the students.
To develop interest of learners, at the end of experiments, questions are also given. The literature required for particular experiments is also given. In case of some experiments, standard results like melting points are also provided.
Considering the depth of students, book is written in very simple language and unnecessary explanation is avoided. The book will definitely generate interest of the learner in understanding and performing the experiments.

CH - 316 : PHYSICAL CHEMISTRY PRACTICAL -I Experiment No. 1 ..............................................................01
Conductometric titration of mixture of acids and hence determine the strength of acids.

Experiment No. 2 ..............................................................05
Determine the degree of hydrolysis and hydrolysis constant of sodium acetate conductometrically.

Experiment No. 3 ..............................................................10
Determine Ecal and pH of buffer solution (Citric acid + Na2HPO4) using quinhydrone electrode.

Experiment No...................................................................15
Determine the pKa and Ka of weak monobasic acid by potentiometric titration.

Experiment No. 5 .............................................................20
Determine the amount of aspirin in the given tablet.

Experiment No. 6 ..............................................................27
Determine the pKa of various mixtures of sodium acetate and acetic acid in solution and hence to find the dissociation constant.

Experiment No. 7 ..............................................................30
To study the kinetics of inversion of cane sugar by polarimeter.

Experiment No. 8 .........................................................................................32
Estimation of Na / K by flame photometer in the given sample.

Experiment No. 9 .............................................................36
Determine the refractive indices of a series of KCl solutions and hence the unknown concentration of the given KCl solution.

Experiment No. 10 ............................................................42
Determine the molar refraction of homologous methyl, ethyl and propylalcohol and show that constancy configuration to molar refraction by –CH2 group.

Experiment No. 11 .............................................................46
Study the hydrolysis of methyl acetate in presence of hydrochloric acid.

Experiment No. 12 ..........................................................49
Determine the energy of activation of the reaction between K2S2O8 and KI. (Equal initial concentration)

Experiment No. 13 ..........................................................55
Investigate the kinetics of iodination of acetone (zero order reaction).

Experiment No. 14 ..........................................................58
Determine the molecular weight of high polymer using its solution of different concentration.

Experiment No. 15 ...........................................................62
Determination of surface tension of a liquid by drop method using stalagmometer.

Experiment No. 16 ..........................................................67
To determine the interfacial tension between benzene and water at room temperature by the drop weight method.

Experiment No. 17 ............................................................70
To plot chemistry graphs using Microsoft Excel.

CH - 317 : ORGANIC CHEMISTRY PRACTICAL-I SEPARATION OF BINARY MIXTURES AND QUALITATIVE
ANALYSIS (Total 08 Mixtures)...............................76 to 104
a) Solid-Solid (6 Mixtures)
b) Solid-Liquid (1 Mixture)
c) Liquid-Liquid (1Mixture)
At least one mixture from each of the following should be given: Acid-Base, Acid-Phenol, Acid-Neutral, Phenol-Base, Phenol-Neutral, Base-Neutral, and Neutral-Neutral. (Solid-solid mixtures must be insoluble in water)

EXTRACTION OF NATURAL PRODUCTS (ANY 02)105 to 114
1. Extraction of Anthocyanin from Hibiscus (Shoe Flower).
2. Extraction of Anthocyanin pigments from Rose Flower
3. Extraction of Lutein from Orange marigold
4. Preparation of Perfume from flowers petals using simple distillation

CH - 319 : INORGANIC CHEMISTRY PRACTICAL-I INORGANIC QUALITATIVE ANALYSIS
(Six binary Mixtures containing common anions)..115 to 140
(Excluding phosphates and borates).

ALLOY ANALYSIS (Any Two)................................................141 to 151
i) Estimation of Zn from Brass alloy.
ii) Estimation of Tin gravimetrically as SnO2 from solder alloy.
iii) Estimation of Copper iodometrically from nichrome alloy.
iv) Determination of iron gravimetrically from stainless steel..

COLORIMETRIC ANALYSIS (ANY TWO)...............152 to 164
i) Colorimetric titration of Cu (II) against EDTA method.
ii) Estimation of Titanium using hydrogen peroxide.
iii) Estimation of iron using thiocyanate method.
iv) To determine the concentration of cobalt in the given solution using
R-nitroso salt by colourimetry.

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