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The book on Handbook of Practical Chemistry for Undergraduates: Volume I in the hands of students learning chemistry at undergraduate level and the teachers of chemistry. The book is written...

  • Name : Handbook of Practical Chemistry for Undergraduates : Volume - I
  • Vendor : Prashant Publication
  • Type : General
  • Manufacturing : May 2026
  • Total Pages : 250 Pages
  • Barcode : 9789377764333

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Handbook of Practical Chemistry for Undergraduates : Volume - I
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The book on Handbook of Practical Chemistry for Undergraduates: Volume I in the hands of students learning chemistry at undergraduate level and the teachers of chemistry. The book is written by keeping in mind curriculum of chemistry prescribed by UGC taught at different levels. In Volume I of handbook, we have tried to cover experiments of first and second year level of students of B. Sc.
Practical chemistry is the core part of curriculum of chemistry. Therefore, we have included about 60 experiments in this handbook. The handbook includes different experiments of physical chemistry, organic chemistry, inorganic chemistry and analytical chemistry. Experiments of organic chemistry include Organic Qualitative Analysis in four steps and in six steps, organic preparations and purification techniques. Experiments of inorganic chemistry include Inorganic Qualitative Analysis and inorganic preparations. Analytical chemistry experiments include volumetric and gravimetric methods of analysis.
The book focuses on understanding the principle involved in different experiments. The experiments include the theory behind experiment, reactions involved, labelled diagrams, procedures, calculations, literature required and results. Preparation of solutions required for each experiment are given in details including quantity of reagents required. Procedures of experiments are simple and given in details considering level of students. Calculations are also given in details. Precautions required are also given wherever necessary. Diagrams are well labelled for better understanding of the students.
To develop interest of learners, at the end of experiments, questions are also given. The literature required for experiments is also given. In case of some experiments, standard results like melting points are also provided.
Considering the depth of students, book is written in very simple language and unnecessary explanation is avoided. It will definitely generate interest of the learner in understanding of the experiments. I hope this book will be useful for the undergraduate students of chemistry.

Physical Chemistry Experiments
1. Determination of integral enthalpy of solution of salts.....1

2. Determination of relative viscosity of liquid A and B by viscometer............. 7

3. Determination of percentage composition (v/v) of given mixture of ethyl alcohol and water by viscometer.......12

4. Determination of surface tension by drop number method of given liquid by using stalagnometer..............15

5. Determination of surface tension of given liquid by drop weight method using stalagnometer.............................19

6. Determination of heat of solution of KNO3 / NH4Cl by water equivalent method.................................................21

7. To determine the equivalent weight of Zn / Mg by Eudiometer method.......28

8. Determination of molecular weight of solute by depression of freezing point method.........................32

9. Determination of molecular weight of non-volatile solute by using Landsberger’s apparatus........................38

10. Determination of critical solution temperature of phenol-water system......43

11. Determination of molecular weight of an organic liquid by steam distillation...................47

12. Measurement of pH of different solutions like aerated drinks, fruit juices, shampoos and soaps using pH-meter..........................49

13. Determination of dissociation constant of weak monobasic acid (CH3COOH) by conductance measurement.............................53

14. Estimation of the amount of Lead present in a solution of Lead Nitrate by conductometric titration with Sodium Sulphate...................................58

15. Determination of solubility and solubility product of sparingly soluble salt conductometrically.......................61

16. Determination of Standard electrode potential of Cu/Cu2+, Ag/Ag+ and Zn/ Zn2+ electrode potentiometrically.........................................66

17. Determination of normality and strength of HCl titrating with standard NaOH potentiometrically...........................74

18. Construction of Daniell cell and to determine thermodynamic parameters ΔG, ΔH, ΔS of the cell......................................78

19. Calibration of volumetric apparatus Pipette/Volumetric flask.....................84

Analytical Chemistry Experiments
1. Preparation of standard 0.1N oxalic acid solution and standardization of NaOH solution..................87

2. Preparation of standard 0.1N K2Cr2O7 solution and standardization of ferrous ammonium sulphate solution....................................89

3. Preparation of standard 0.1N NaCl solution and standardization of AgNO3 solution...........................92

4. Preparation of standard 0.1N ZnSO4 solution and standardization of EDTA solution..............................95

5. To standardize commercial sample of HCl using Borax and to write material safety data of the chemicals involved...............................99

6. Preparation of standard 0.1 N Na2CO3 solution and standardization of HCl solution....................102

7. Preparation of standard 0.1 N oxalic acid solution and standardization of KMnO4 solution.................................105

8. Preparation of std.0.1 N Na2S2O3 solution and estimation of Cu (II) ionsiodometrically........................108

9. Determination of total hardness of water sample.........110

10. Preparation of std. 0.05 N potassium hydrogen phthalate solution and standardization of NaOH solution......................................114

11. Preparation of standard 0.1 N K2Cr2O7 (or Potassium dichromate) and standardization of Na2S2O3 solution.............................117

12. Estimation of aniline / phenol...............................120

13. Estimation of acetic acid in commercial vinegar using NaOH solution.....124

14. Estimation of aspirin in the given drug sample..........127

15. Estimation of alkali content in antacid tablet using HCl...................130

16. Determination of volume strength of H2O2...............134

17. Estimation of chlorides by Mohr’s method.........138

18. Estimation of Fe (II) by redox titration with KMnO4....142

19. Estimation of copper iodometrically.........145

20. Estimation of Mg2+ by complexometric titration with EDTA.....................149

21. Determination of dissolved oxygen (DO) in water sample................153

22. Determination of loss per gram and percentage purity of Zinc Carbonate gravimetrically........................158

23. Estimation of nickel as nickel dimethyl glyoxime gravimetrically..............160

24. Estimation of barium as barium sulphate gravimetrically.........................163

25. Estimation of lead as lead chromate PbCrO4 (By Gooch
crucible method)....................166

26. Separation of mixture of o-nitro aniline and p-nitro aniline by Thin Layer Chromatography and to determine their Rf values.................168

27. Separation of mixture of any two amino acids by paper
chromatography.....................................171

Organic Qualitative Analysis
1. Analysis of given organic compound in 4 stages ........175
I) Type determination
II) Preliminary tests
III) Determination of physical constant
IV) Identification of functional group

2. Analysis of given organic compound in 6 stages........190
I) Type determination
II) Preliminary tests
III) Determination of physical constant
IV) Detection of elements (Sodium fusion test)
V) Identification of functional group
VI) Determination of structure

Organic Preparations
1. Aniline to acetanilide by using Zn/Acetic acid............212

2. Semicarbazone derivative of Aldehydes / Ketones....213

3. Benzoyl derivative of Ar–NH2 / Ar–OH group..214

4. Acetanilide to p-bromo acetanilide using ceric ammonium nitrate............216

5. To prepare Benzoic acid from benzamide.........217

Purification Techniques
1. Purification of given organic compound by sublimation............................219

2. Purification of given organic compound by recrystallisation.....................220

3. Purification of given organic liquid by distillation.....................................222

Inorganic Qualitative Analysis
1. Analysis of inorganic compound containing one basic radical (cation) and one acidic radical (anion)......229

Inorganic Preparations
1. Preparation of Tetramine Copper (II) sulfate monohydrate.......................244

2. Preparation of Hexamine nickel (II) chloride [Ni(NH3)6]Cl2....................246

3. Preparation of Ferrous Ammonium Sulfate (Mohr’s salt)..........................248

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